冯继文 , 贺玉贵 , 黄重阳 , 张震 , 刘朝阳 . 微波诱导光学核极化进展[J]. 波谱学杂志, 2017 , 34(2) : 231 -244 . DOI: 10.11938/cjmr20170213

[1] GERSHENFELD N A, CHUANG I L. Bulk spin-resonance quantum computation[J]. Science, 1997, 275(5298):350-356.
[2] PENG X H, SUTER D. Spin qubits for quantum simulations[J]. Front Phys China, 2010, 5(1):1-25.
[3] LI Z K, ZHOU H, JU C Y, et al. Experimental realization of a compressed quantum simulation of a 32-spin Ising chain[J]. Phys Rev Lett, 2014, 112(22):220501.
[4] VLAARDINGERBROEK M T, BOER J A. Magnetic resonance imaging[M]. 2nd ed. Berlin:Springer-Verlag, 1999.
[5] TAKEDA K. Studies on dynamic nuclear polarization using photo-excited triplet electron spins[D]. Kyoto:Kyoto University, 2003.
[6] CHERUBINI A, PAYNE G, LEACH M, et al. Hyperpolarising ¹³C for NMR studies using laser-polarised 129Xe:SPINOE vs thermal mixing[J]. Chem Phys Lett, 2003, 371(5):640-644.
[7] LI H D, ZHAN Z Y, HAN Y Q, et al. Lung MRI use Hyperpolarized gase[J]. Chinese J Magn Reson, 2014, 31(3):307-320. 李海东, 张智颖, 韩叶清, 等. 超级化气体肺部磁共振成像[J]. 波谱学杂志, 2014, 31(3):307-320.
[8] GOLMAN K, AXELSSON O, JÓHANNESSON H, et al. Parahydrogen-induced polarization in imaging:Subsecond ¹³C angiography[J]. Magn Reson Med, 2001, 46(1):1-5.
[9] BLÄTTLER C, JENT F, PAUL H. A novel radical-triplet pair mechanism for chemically induced electron polarization (CIDEP) of free radicals in solution[J]. Chem Phys Lett, 1990, 166(4):375-380.
[10] OVERHAUSER A W. Paramagnetic relaxation in metals[J]. Physical Review, 1953, 89(4):689-790.
[11] LUMATA L L, MARTIN R, JINDAL A K, et al. Development and performance of a 129-GHz dynamic nuclear polarizer in an ultra-wide bore superconducting magnet[J]. MAGMA, 2015, 28(2):195-205.
[12] POLYON C, LURIE D, YOUNGDEE W, et al. Field-cycled dynamic nuclear polarization (FC-DNP) of ¹⁴N and ¹⁵N nitroxide radicals at low magnetic field[J]. J Phys D Appl Phys, 2007, 40(18):5527-5532.
[13] NEUDERT O, MATTEA C, STAPF S, et al. Fast-field-cycling relaxometry enhanced by dynamic nuclear polarization[J]. Micropor Mesopor Mat, 2015, 205:70-74.
[14] JANNIN S, COMMENT A, KURDZESAU F, et al. A 140 GHz prepolarizer for dissolution dynamic nuclear polarization[J]. J Chem Phys, 2008, 128(24):241102.
[15] JANNIN S, BORNET A, COLOMBO S, et al. Low-temperature cross polarization in view of enhancing dissolution dynamic nuclear polarization in NMR[J]. Chem Phys Lett, 2011, 517(4):234-236.
[16] HAZE O, CORZILIUS B R, SMITH A A, et al. Water-soluble narrow-line radicals for dynamic nuclear polarization[J]. J Am Chem Soc, 2012, 134(35):14287-14290.
[17] ZHOU J W, LI L Y, HU H B, et al. Study of natural diamonds by dynamic nuclear polarization-enhanced ¹³C nuclear magnetic resonance spectroscopy[J]. Solid State Nucl Magn Reson, 1994, 3(6):339-351.
[18] HE Y G, FENG J W, ZHANG Z, et al. Development of pulsed dynamic nuclear polarization for enhancing NMR and MRI[J]. Chinese J Magn Reson, 2015, 32(2):393-398. 贺玉贵, 冯继文, 张志, 等. 脉冲动态核极化增强的NMR和MRI系统研究[J]. 波谱学杂志, 2015, 32(2):393-398.
[19] HE Y G, FENG J W, ZHANG Z, et al. A peripheral component interconnect express-based scalable and highly integrated pulsed spectrometer for solution state dynamic nuclear polarization[J]. Rev Sci Instrum, 2015, 86(8):083101.
[20] HE Y G, ZHANG Z, FENG J W, et al. Simultaneous acquisition of multi-nuclei enhanced NMR/MRI by solution state dynamic nuclear polarization[J]. Sci China Chem, 2016, 59(7):830-835.
[21] MAIER G, HAEBERLEN U, WOLF H, et al. Optische kernspin-polarisation in anthracen-kristallen[J]. Phys Lett A, 1967, 25(5):384-385.
[22] GROVER B. Noble-gas NMR detection through noble-gas-rubidium hyperfine contact interaction[J]. Phys Rev Lett, 1978, 40(6):391-392.
[23] JEFFRIES C. Some new schemes for polarizing nuclei[J]. Phys Rev Lett, 1967, 19(21):1221-1224.
[24] LAMPEL G. Nuclear dynamic polarization by optical electronic saturation and optical pumping in semiconductors[J]. Phys Rev Lett, 1968, 20(10):491-493.
[25] DEIMLING M, BRUNNER H, DINSE K, et al. Microwave-induced optical nuclear polarization (MI-ONP)[J]. J Magn Reson, 1980, 39(2):185-202.
[26] HENSTRA A, LIN T S, SCHMIDT J, et al. High dynamic nuclear polarization at room temperature[J]. Chem Phys Lett, 1990, 165(1):6-10.
[27] KAGAWA A, NEGORO M, TAKEDA K, et al. Magnetic-field cycling instrumentation for dynamic nuclear polarization-nuclear magnetic resonance using photoexcited triplets[J]. Rev Sci Instrum, 2009, 80(4):044705.
[28] ⅡNUMA M. Dynamic nuclear polarization at high temperature for polarized proton target[D]. Kyoto:Kyoto University, 1997.
[29] ⅡNUMA M, TAKAHASHI Y, SHAKÉ I, et al. High proton polarization by microwave-induced optical nuclear polarization at 77 K[J]. Phys Rev Lett, 2000, 84(1):171.
[30] BLOEMBERGEN N. On the interaction of nuclear spins in a crystalline lattice[J]. Physica, 1949, 15(3):386-426.
[31] KAGAWA A, MUROKAWA Y, TAKEDA K, et al. Optimization of ¹H spin density for dynamic nuclear polarization using photo-excited triplet electron spins[J]. J Magn Reson, 2009, 197(1):9-13.
[32] HENSTRA A, DIRKSEN P, SCHMIDT J, et al. Nuclear spin orientation via electron spin locking (NOVEL)[J]. J Magn Reson, 1988, 77(2):389-393.
[33] HAUSSER K. Optical spin polarization in molecular crystals[J]. Pure Appl Chem, 1972, 32(1-4):183-196.
[34] YANG T C, SLOOP D J, WEISSMAN S, et al. Zero-field magnetic resonance of the photo-excited triplet state of pentacene at room temperature[J]. J Chem Phys, 2000, 113(24):11194-11201.
[35] SLOOP D J, YU H L, LIN T S, et al. Electron spin echoes of a photoexcited triplet:Pentacene in p-terphenyl crystals[J]. J Chem Phys, 1981, 75(8):3746-3757.
[36] TAKEDA K, TAKEGOSHI K, TERAO T. Dynamic nuclear polarization by electron spins in the photoexcited triplet state:Ⅱ. High polarization of the residual protons in deuterated naphthalene[J]. J Phys Soc Jpn, 2004, 73(8):2319-2322.
[37] MCCONNELL H M, CHESNUT D B. Theory of isotropic hyperfine interactions in π-electron radicals[J]. J Chem Phys, 1958, 28(1):107-117.
[38] WENCKEBACH W T. The solid effect[J]. Appl Magn Reson, 2008, 34(3, 4):227-235.
[39] TAKEDA K, TAKEGOSHI K, TERAO T. Dynamic nuclear polarization by electron spins in the photoexcited triplet state:I. Attainment of proton polarization of 0.7 at 105 K in naphthalene[J]. J Phys Soc Jpn, 2004, 73(8):2313-2318.
[40] VAN KESTEREN H, WENCKEBACH W T, SCHMIDT J. The mechanism of microwave-induced optical nuclear polarization in fluorene doped with phenanthrene:A qualitative analysis[J]. Chem Phys Lett, 1985, 121(4):440-445.
[41] VAN KESTEREN H, WENCKEBACH W T, SCHMIDT J. The mechanism of microwave induced optical nuclear polarization in the system fluorene doped with phenanthrene:A quantitative analysis[J]. Mol Phys, 1986, 58(2):263-271.
[42] PENFOLD J, WARD R, WILLIAMS W. A time-of-flight neutron reflectometer for surface and interfacial studies[J]. J Phys E Sci Instrum, 1987, 20(11):1411-1417.
[43] VERHEIJ P F, WENCKEBACH W T, SCHMIDT J. Microwave induced optical nuclear polarization at 75 GHz:A quantitative analysis[J]. Appl Magn Reson, 1993, 5(2):187-205.
[44] EICHHORN T R, HAAG M, VAN DEN BRANDT B, et al. An apparatus for pulsed ESR and DNP experiments using optically excited triplet states down to liquid helium temperatures[J]. J Magn Reson, 2013, 234:58-66.
[45] EICHHORN T, BRANDT BVD, HAUTLE P, et al. Dynamic nuclear polarisation via the integrated solid effect Ⅱ:experiments on naphthalene-h 8 doped with pentacene-d¹⁴[J]. Mol Phys, 2014, 112(13):1773-1782.
[46] ⅡNUMA M, SHAKÉ I, TAKIZAWA R, et al. High proton polarization in crystalline naphthalene by dynamic nuclear polarization with laser excitation at room temperature and liquid nitrogen temperature[J]. Phys Lett A, 1995, 208(3):251-256.
[47] TAKEDA K, YAMAMURA T, KAGAWA A, et al. Enhancement of efficiency in photo-excitation to the triplet state by laser-pulse reshaping[J]. J Magn Reson, 2005, 174(2):310-313.
[48] TAKEDA K, TAKEGOSHI K, TERAO T. Zero-field electron spin resonance and theoretical studies of light penetration into single crystal and polycrystalline material doped with molecules photoexcitable to the triplet state via intersystem crossing[J]. J Chem Phys, 2002, 117(10):4940-4946.
[49] ALLGEIER J, BUNTKOWSKY G, HENTRICH S, et al. Optical nuclear polarization of deuterium spins:mechanisms and applications in solid state NMR[J]. Isr J Chem, 1992, 32(2, 3):205-213.
[50] TAKEDA K, TAKEGOSHI K, TERAO T. Dynamic nuclear polarization by photoexcited-triplet electron spins in polycrystalline samples[J]. Chem Phys Lett, 2001, 345(1):166-170.
[51] TATEISHI K, NEGORO M, KAGAWA A, et al. Hyperpolarization of thin films with dynamic nuclear polarization using photoexcited triplet electrons[J]. J Phys Soc Jpn, 2013, 82(8):084005.
[52] TATEISHI K, NEGORO M, KAGAWA A, et al. Dynamic nuclear polarization with photoexcited triplet electrons in a glassy matrix[J]. Angew Chem, 2013, 125(50):13549-13552.
[53] SAKAGUCHI S, UESAKA T, KAWAHARA T, et al. Proton polarization in photo-excited aromatic molecule at room temperature enhanced by intense optical source and temperature control[J]. Nuclear Instru and Meth Phys Res B:Beam Interactions with Materials and Atoms, 2013, 317:679-684.
[54] KAWAHARA T, SAKAGUCHI S, TATEISHI K, et al. Kinetic parameters of photo-excited triplet state of pentacene determined by dynamic nuclear polarization[J]. J Phys Soc Jpn, 2015, 84(4):044005.
[55] TATEISHI K, NEGORO M, NISHIDA S, et al. Room temperature hyperpolarization of nuclear spins in bulk[J]. P Natl Acad Sci USA, 2014, 111(21):7527-7530.
[56] NEGORO M, NAKAYAMA K, TATEISHI K, et al. ²H-decoupling-accelerated ¹H spin diffusion in dynamic nuclear polarization with photoexcited triplet electrons[J]. J Chem Phys, 2010, 133(15):154504.
[57] EICHHORN T, HAAG M, VAN DEN BRANDT B, et al. High proton spin polarization with DNP using the triplet state of pentacene-d¹⁴[J]. Chem Phys Lett, 2013, 555:296-299.
[58] ⅡNUMA M, TAKAHASHI Y, SHAKÉ I, et al. Proton polarization with p-terphenyl crystal by integrated solid effect on photoexcited triplet state[J]. J Magn Reson, 2005, 175(2):235-241.
[59] PINES A, GIBBY M, WAUGH J. Proton-enhanced NMR of dilute spins in solids[J]. J Chem Phys, 1973, 59(2):569-590.