用红外吸收光谱、紫外吸收光谱、核磁共振(NMR)波谱(包含1H NMR、13C NMR、DEPT135、1H-1H COSY、1H-13C HMQC和1H-13C HMBC)、质谱、差示扫描量热分析、X-射线粉末衍射和元素分析等方法对卢立康唑进行了结构分析.对卢立康唑所有的1H和13C NMR信号进行了归属,并通过多种谱学技术确证了卢立康唑的结构.
Infrared spectra, ultraviolet spectra, nuclear magnetic resonance (NMR) spectra (i.e., 1H NMR, 13C NMR, DEPT135, 1H-1H COSY, 1H-13C HMQC and 1H-13C HMBC) and mass spectra of luliconazole were collected and used to characterize the compound. Differential scanning calorimetry, X-ray power diffraction and elementary analysis were also performed. All 1H and 13C NMR signals of the compound were assigned. The structure of the compound was determined.
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