谱仪研制技术进展专栏

TM110模式DNP探头的研制与应用

  • 陶泉 ,
  • 贺玉贵 ,
  • 王超 ,
  • 冯继文 ,
  • 陈方 ,
  • 刘朝阳
展开
  • 1. 波谱与原子分子物理国家重点实验室, 武汉磁共振中心(中国科学院 武汉物理与数学研究所), 湖北 武汉 430071;
    2. 中国科学院大学, 北京 100049;
    3. 武汉光电国家实验室(筹), 华中科技大学 光学与电子信息学院, 湖北 武汉 430074
陶泉(1990-),男,贵州遵义人,硕士研究生,无线电物理专业.

收稿日期: 2015-05-06

  修回日期: 2016-01-23

  网络出版日期: 2016-03-05

基金资助

国家重大科研装备研制项目(ZDYZ2010-2),国家自然科学基金资助项目(11405264),国家重大科学仪器设备开发专项资助项目(2011YQ120035).

A TM110 Dynamic Nuclear Polarization Probe: Design and Applications

  • TAO Quan ,
  • HE Yu-gui ,
  • WANG Chao ,
  • FENG Ji-wen ,
  • CHEN Fang ,
  • LIU Chao-yang
Expand
  • 1. State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, National Center for Magnetic Resonance in Wuhan (Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences), Wuhan 430071, China;
    2. University of Chinese Academy of Sciences, Beijing 100049, China;
    3. Wuhan National Laboratory for Optoelectronics, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, China

Received date: 2015-05-06

  Revised date: 2016-01-23

  Online published: 2016-03-05

摘要

为了满足自主研发的X波段动态核极化系统(DNP-NMR/MRI)对探头的需求,设计制作了用于动态核极化的TM110模式圆柱形谐振腔探头.通过理论分析计算得到了探头腔体的初步尺寸,进而利用软件对其完整结构做进一步的仿真优化,并测试了基于优化参数设计加工的探头的性能参数.完成了探头在自主研制的场强为0.35 T的DNP-NMR/MRI系统上的测试,得到了大于50倍信噪比(S/N)增强的质子信号,同时获得信噪比增强的磁共振影像.

本文引用格式

陶泉 , 贺玉贵 , 王超 , 冯继文 , 陈方 , 刘朝阳 . TM110模式DNP探头的研制与应用[J]. 波谱学杂志, 2016 , 33(1) : 44 -53 . DOI: 10.11938/cjmr20160104

Abstract

A cylindrical cavity working in TM110 mode at the X-band frequencies was designed and manufactured for dynamic nuclear polarization (DNP) systems. The dimensions of the cavity were theoretically calculated, and then optimized with the software Ansoft-HFSS. The fabricated probe was tested experimentally on a homebuilt DNP system. With the probe,1H NMR signal was acquired with more than 50-folds of sensitivity enhancement; and a clear DNP-enhanced image was obtained.

参考文献

[1] Krummenacker J G. Dynamic Nuclear Polarization for Magnetic Resonance Imaging: An In-bore Approach[D]. Frankfurt: University of Frankfurt, 2012.

[2] Overhauser A W. Polarization of nuclei in metals[J]. Phys Rev, 1953, 92(2): 411-415.

[3] Maly T, Debelouchina G T, Bajaj V S, et al. Dynamic nuclear polarization at high magnetic fields[J]. J Chem Phys, 2008, 128(5): 052211.

[4] Kay C W M, Grishin Y A, Weber S, et al. An improved TM110 resonator for continuous-wave ENDOR studies at X-band[J]. Appl Magn Reson, 2007, 31(3): 599-609.

[5] Christidis T C, Heineken F W. A cylinder TM110 ENDOR cavity[J]. J Phys E: Sci Instrum, 1985, 18(4): 281-283.

[6] Christidis T C, Heineken F W. A microwave cavity for high power ENDOR spectroscopy[J]. J Phys E: Sci Instrum, 1972, 6(5): 432-434.

[7] Chacko V P. “Wonderstone” ENDOR cavity[J]. Rev Sci Instrum, 1978, 49(7): 1 012-1 014.

[8] Lu Jing-fen(卢景雰). Advanced Electron Paramagnetic Resonance Spectroscopy and Its Applications(现代电子顺磁共振波谱学及其应用)[M]. Beijing(北京): Peking University Press(北京大学出版社), 2012.

[9] Liao Cheng-en(廖承恩). Basis of Microwave Technique(微波技术基础)[M]. Xian(西安): Xidian University Press(西安电子科技大学出版社), 1994.

[10] Zhang K Q, Li D J. Electromagnetic Theory for Microwaves and Optoelectronics (2nd) [M]. Berlin: Springer-Verlag, 2007.

[11] Wang Wen-xiang(王文祥). Microwave Engineering Technology(微波工程基础)[M]. Beijing(北京): National Defense Industry Press(国防工业出版社), 2009.

[12] Mao Wen-ping(毛文平). Hardware Development for High-Field NMR(高场核磁共振波谱仪硬件的研究)[D]. Wuhan(武汉): Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences(中国科学院武汉物理与数学研究所), 2012.

[13] Wen Xu-jie(温旭杰), Huang Pu(黄璞), Geng Jian-pei(耿建培), et al. Design of rectangular and planar microresonators for X-band pulsed EPR spectrometer (X波段脉冲电子顺磁共振谱仪的矩形谐振腔与微型平面腔的设计)[J]. Chinese J Magn Reson(波谱学杂志), 2011, 28(4): 437-446.

文章导航

/