Chinese Journal of Magnetic Resonance ›› 1984, Vol. 1 ›› Issue (4): 319-325.
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Li Liyun, Qiu Hanging, La Xiaoming, Yuan Hanzhen, Shen Lianfang
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Abstract: In this paper,1H 13C, 31P NMR spectra of 6 phosphoramidothiolates of genera formula H2N RS P=O-O-COOR'(R=methyl, ethyl, isopropyl,propyl;R'=methyl, ethyl, isopropyl) and two-dimensional 13C-1H heteronuclear chemical shift correlation NMR spectroscopy were recorded. 1H,13C, 31P chemical shifts and 1H-1H,31P-1H,31P-13C different kinds of coupling contant were determined. The relations between of NMR parameters and molecular motion and between 31P chemical shifts and the insecticidal activity were discussed.
Li Liyun, Qiu Hanging, La Xiaoming, Yuan Hanzhen, Shen Lianfang. NMR STUDY ON S-ALKYL-O-(O-ALKOXYCARBONYLPHENYL) PHOSPHORAMIDOTHIOLATE[J]. Chinese Journal of Magnetic Resonance, 1984, 1(4): 319-325.
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http://magres.apm.ac.cn/EN/Y1984/V1/I4/319