PRECISE MEASUREMENTS OF 13C-1H DIPOLAR SPECTRA UNDER SLOW MAGIC ANGLE SPINNING

Chinese Journal of Magnetic Resonance

Previous Articles Next Articles

PRECISE MEASUREMENTS OF ¹³C-¹H DIPOLAR SPECTRA UNDER SLOW MAGIC ANGLE SPINNING

SHEN Yi-min1～4, CHEN Shi-ming1*, LIU Wu-yang2, JIN Gui-dong1，HORII Fumilaka3

1.Center of Analysis and Measurement, Fudan University, Shanghai 200433, China; 2.Laboratory of Magnetic Resonance and Atomic and Molecular Physics, and Mathem atics, Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences, Wuhan 430071, China; 3.Institute for Chemical Research, Kyoto University, Kyoto 611-0011, Japan; 4.Department of Radiology, Wayne State University School of Medicine, Detroit, MI 48201, USA

Received:2002-07-12 Revised:2002-09-04 Published:2003-03-05 Online:2003-03-05
About author:沈伊民（1961-），男，江苏江阴人，副教授，博士，现从事医学核磁共振影像学及波谱学研究.
Supported by:
This work was financially supported by grant from the NSFC(29974006), by the SRF for the ROCS from the SEM and by the Laboratory of MRAMP.

Abstract

CLC Number:

O482.53

SHEN Yi-min1～4, CHEN Shi-ming1*, LIU Wu-yang2, JIN Gui-dong1，HORII Fumilaka3.

PRECISE MEASUREMENTS OF ¹³C-¹H DIPOLAR SPECTRA UNDER SLOW MAGIC ANGLE SPINNING

[J]. Chinese Journal of Magnetic Resonance.

［１］　ＳｃｈａｅｆｅｒＪ，ＭｃｋａｙＲＡ，ＳｔｅｊｓｋａｌＥＯ，at al．ＤｉｐｏｌａｒＲｏｔａｔｉｏｎａｌＳｐｉｎＥｃｈｏＣ１３ＮＭＲｏｆＰｏｌｙｍｅｒｓ［Ｊ］．ＪＭａｇｎ

Ｒｅｓｏｎ，１９８３，５２：１２３．

［２］　ＨｅｒｚｆｅｌｄＪ，ＢｅｒｇｅｒＡＥ．ＳｉｄｅｂａｎｄＩｎｔｅｎｓｉｔｉｅｓｉｎＮＭＲＳｐｅｃｔｒａｏｆＳａｍｐｌｅｓＳｐｉｎｎｉｎｇａｔｔｈｅＭａｇｉｃＡｎｇｌｅ［Ｊ］．Ｊ

ＣｈｅｍＰｈｙｓ，１９８０，７３：６０２１．

［３］　ＳｈｅｎＹ，ＫａｊｉＨ，ＨｏｒｉｉＦ．Ａｎａｎａｌｙｔｉｃａｌｅｘｐｒｅｓｓｉｏｎｏｆｍａｇｉｃａｎｇｌｅｓｐｉｎｎｉｎｇｎｕｃｌｅａｒｍａｇｎｅｔｉｃｒｅｓｏｎａｎｃｅｆｒｅｅｉｎ

ｄｕｃｔｉｏｎｄｅｃａｙｉｎｔｗｏｓｉｔｅｅｘｃｈａｎｇｅｐｒｏｂｌｅｍ［Ｊ］．ＣｈｉｎｅｓｅＰｈｙｓｉｃｓＬｅｔｔｅｒｓ，１９９８，１５（６）：４５３；ＣｈｉｎｅｓｅＪＭａｇｎ

Ｒｅｓｏｎ，１９９９，１６（６）：４８５．

［４］　ＢｉｅｌｅｃｋｉＡ，ＫｏｌｂｅｒｔＡＣ，ＬｅｖｉｔｔＭＨ．ＦｒｅｑｕｅｎｃｙＳｗｉｔｃｈｅｄＰｕｌｓｅＳｅｑｕｅｎｃｅｓＨｏｍｏｎｕｃｌｅａｒＤｅｃｏｕｐｌｉｎｇａｎｄＤｉｌｕｔｅ

ＳｐｉｎＮＭＲｉｎＳｏｌｉｄｓ［Ｊ］．ＣｈｅｍＰｈｙｓＬｅｔｔ，１９８９，１５５（４，５）：３４１．

［５］　ＮａｋａｉＴ，ＴｅｒａｏＴ．ＭｅａｓｕｒｅｍｅｎｔｓｏｆＨｅｔｅｒｏｎｕｃｌｅａｒＤｉｐｏｌａｒＰｏｗｄｅｒＰａｔｔｅｒｎｓＤｕｅＯｎｌｙｔｏＤｉｒｅｃｔｌｙＢｏｎｄｅｄＣｏｕ

ｐｌｉｎｇｓ［Ｊ］．ＭａｇｎＲｅｓｏｎＣｈｅｍ，１９９２，３０：４２．

［６］　ＨｏｎｇＭ，ＳｃｈｍｉｄｔＲｏｈｒＫ，ＰｉｎｅｓＡ．ＮＭＲＭｅａｓｕｒｅｍｅｎｔｏｆＳｉｇｎｓａｎｄＭａｇｎｉｔｕｄｅｓｏｆＣＨＤｉｐｏｌａｒＣｏｕｐｌｉｎｇｓｉｎ

Ｌｅｃｉｔｈｉｎ［Ｊ］．ＪＡｍＣｈｅｍＳｏｃ，１９９５，１１７：３３１０．

［７］　ＳｃｈｍｉｄｔＲｏｈｒＫ，ＣｌａｕｓｓＪ，ＳｐｉｅｓｓＨＷ．ＣｏｒｒｅｌａｔｉｏｎｏｆＳｔｒｕｃｔｕｒｅ，Ｍｏｂｉｌｉｔｙ，ａｎｄＭｏｒｐｈｏｌｏｇｉｃａｌＩｎｆｏｒｍａｔｉｏｎｉｎ

ＨｅｔｅｒｏｇｅｎｅｏｕｓＰｏｌｙｍｅｒＭａｔｅｒｉａｌｓｂｙ２ＤｉｍｍｅｎｓｉｏｎａｌＷｉｄｅｌｉｎｅＳｅｐａｒａｔｉｏｎＮＭＲＳｐｅｃｔｒｏｓｃｏｐｙ［Ｊ］．Ｍａｃｒｏｍｏｌｅ

ｃｕｌｅｓ，１９９２，２５：３２７３．

[1]	XU Xiaojie, CHEN Yan’an, LI Xufei, ZHANG Yuncai, ZHANG Yong, ZHAN Dongkai, PAN Ting. Structural Elucidation of Hybutimibe [J]. Chinese Journal of Magnetic Resonance, 2024, 41(1): 43-55.
[2]	CHEN Yang, ZHOU Meng, LI Yong, YANG Haijun. Independent Development of Sample Preparation Tools for Solid-state NMR [J]. Chinese Journal of Magnetic Resonance, 2024, 41(1): 77-86.
[3]	HU Xiaoyang, LIU Ying, CHEN Shu, DONG Binbin. Fusing Attention Mechanism with Mask RCNN for Recognition of Acoustic Neuroma and Meningioma in Cerebellopontine Angle [J]. Chinese Journal of Magnetic Resonance, 2023, 40(3): 293-306.
[4]	ZHAI Chonggang,WANG Pengcheng,SHAN Yubao,LAN Yu,HU Rui,YANG Yunhuang. Structure Characterization and Analgesic Activity of Novel Pyrazolo[3,4-d]pyrimidin-4-one Derivatives [J]. Chinese Journal of Magnetic Resonance, 2023, 40(1): 1-9.
[5]	Ya-ting GU, Wen-na ZHANG, Jing-feng HAN, Cai-yi LOU, Hui-hui CHEN, Shu-tao XU, Ying-xu WEI, Zhong-min LIU. Investigation on the Differences of the Alcohols Conversion over H-SAPO-34 Zeolite [J]. Chinese Journal of Magnetic Resonance, 2022, 39(4): 428-438.
[6]	Han-wei WANG,Hao WU,Jing TIAN,Jun-feng ZHANG,Peng ZHONG,Li-zhao CHEN,Shu-nan WANG. The Diagnostic Value of Quantitative Parameters of T₂/FLAIR Mismatch Sign in Evaluating the Molecular Typing of Lower-grade Gliomas [J]. Chinese Journal of Magnetic Resonance, 2022, 39(1): 56-63.
[7]	LIU Ying, CHEN Jing-cong, HU Xiao-yang, ZHANG Hao-wei. Classification and Localization of Meningioma and Acoustic Neuroma in Cerebellopontine Angle Based on Mask RCNN [J]. Chinese Journal of Magnetic Resonance, 2021, 38(1): 58-68.
[8]	HE Ke-liang, ZHANG Wei-qun, Lin Chuan-fu. Design of the Atomic Storage Time of a Miniaturized Hydrogen Maser [J]. Chinese Journal of Magnetic Resonance, 2020, 37(2): 200-208.
[9]	ZHANG Yi-ming, CHEN Zhi-xue, YANG Xiao-yun. Spectral Analyses and Structural Elucidation of Cyflumetofen [J]. Chinese Journal of Magnetic Resonance, 2020, 37(2): 224-231.
[10]	WANG Jia-xin, FENG Ji-wen, CHEN Jun-fei, WANG Li-ying, LIU Chao-yang. Design and Fabrication of a Magic-Angle Spinning Rotor for Solid-State Nuclear Magnetic Resonance Probe [J]. Chinese Journal of Magnetic Resonance, 2019, 36(4): 446-455.
[11]	WANG Hong-zhi, WANG Shen-lin, HU Bin-wen, YU Yi-hua, SONG Yi-qiao, YAO Ye-feng. A Virtual NMR Spectrometer Based on Numerical Computational Simulations [J]. Chinese Journal of Magnetic Resonance, 2019, 36(3): 288-297.
[12]	LIN Yun-liang, GAO Hong-mei, LI Feng, CHEN Xiang-feng. Spectral Analysis and Structural Elucidation of Luliconazole [J]. Chinese Journal of Magnetic Resonance, 2018, 35(3): 385-392.
[13]	JIANG Dan, WANG Wei, BI Qian-nan, SU Dan-dan. Spectral Analysis of a 1,4-Thiazinamide FKBPs Ligand [J]. Chinese Journal of Magnetic Resonance, 2018, 35(2): 204-214.
[14]	JI Xiao-long, YU Shui-tao, CHEN Zai-xin. Spectral Analyses of Ecabet Sodium [J]. Chinese Journal of Magnetic Resonance, 2018, 35(1): 109-118.
[15]	SUN Yi, CHEN Yan-ke, LI Jian-ping, ZHAO Yong-xiang, YANG Jun. Efficiency of Double Cross Polarization in Magic-Angle Spinning Solid-State NMR Studies on Membrane Proteins [J]. Chinese Journal of Magnetic Resonance, 2017, 34(3): 257-265.

PRECISE MEASUREMENTS OF ¹³C-¹H DIPOLAR SPECTRA UNDER SLOW MAGIC ANGLE SPINNING

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments