Spectral Analysis and Structural Elucidation of Triptophnolide

  • DAI Zhong ,
  • ZHANG Yu-mei ,
  • HE Yi ,
  • MA Shuang-cheng ,
  • WANG Fei-fei ,
  • LIU Bin
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  • 1. National Institutes for Food and Drug Control, Beijing 100050, China;
    2. School of Chinese Materia Medica, Beijing University of Chinese Medicine, Beijing 100029, China

Received date: 2015-11-21

  Revised date: 2017-01-04

  Online published: 2017-03-05

Abstract

Ultraviolet (UV) spectrum, infrared (IR) spectrum, mass (MS) spectra and nuclear magnetic resonance (NMR) spectra (i.e., 1H NMR, 13C NMR, DEPT, 1H-1H COSY, NOE, 1H-13C HSQC and 1H-13C HMBC) of Triptophnolide were collected and interpreted. All 1H and 13C NMR signals were assigned. Base on the data, the structure of reference standard Triptophnolide was determined.

Cite this article

DAI Zhong , ZHANG Yu-mei , HE Yi , MA Shuang-cheng , WANG Fei-fei , LIU Bin . Spectral Analysis and Structural Elucidation of Triptophnolide[J]. Chinese Journal of Magnetic Resonance, 2017 , 34(1) : 35 -42 . DOI: 10.11938/cjmr20170105

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