固体核磁共振技术在锡硅分子筛表征中的应用
肖瑶1,2,夏长久3,易先锋1,*(
),刘凤庆1,2,刘尚斌4,郑安民1,*()
),刘凤庆1,2,刘尚斌4,郑安民1,*()
Progress in the Studies on Sn-Zeolites by Solid-State Nuclear Magnetic Resonance
Yao XIAO1,2,Chang-jiu XIA3,Xian-feng YI1,*(),Feng-qing LIU1,2,Shang-bin LIU4,An-min ZHENG1,*()
),Feng-qing LIU1,2,Shang-bin LIU4,An-min ZHENG1,*()
图11. (A) (a, c)葡萄糖和(b, d)果糖分别吸附在(a, b)Si-Beta和(c, d) Sn-Beta分子筛上的13C MAS NMR谱图.(B)果糖吸附在Sn-Beta分子筛上不同CP接触时间[(a) 0.1 ms, (b) 1.0 ms, (c)无CP]的CP MAS NMR谱图（根据文献[
Fig.11. (A) 13C MAS NMR of (a) glucose adsorbed into Si-Beta, (b) fructose adsorbed into Si-Beta, (c) glucose adsorbed into Sn-Beta, (d) fructose adsorbed into Sn-Beta. (B) Spectra from fructose adsorbed into Sn-Beta: (a) CP contact time of 0.1 ms; (b) CP contact time of 1.0 ms; and (c) no CP (Reproduced from Ref. [
