固体核磁共振技术在锡硅分子筛表征中的应用
肖瑶1,2,夏长久3,易先锋1,*(
),刘凤庆1,2,刘尚斌4,郑安民1,*()
),刘凤庆1,2,刘尚斌4,郑安民1,*()
Progress in the Studies on Sn-Zeolites by Solid-State Nuclear Magnetic Resonance
Yao XIAO1,2,Chang-jiu XIA3,Xian-feng YI1,*(),Feng-qing LIU1,2,Shang-bin LIU4,An-min ZHENG1,*()
),Feng-qing LIU1,2,Shang-bin LIU4,An-min ZHENG1,*()
图8. Si-Beta分子筛以及各种锡硅分子筛(a)吸附TMPO的31P NMR谱图、(b)吸附2-13C-丙酮的13C CP MAS NMR谱图、(c)吸附NH3的1H NMR谱图及差谱（根据文献[
Fig.8. (a) 31P MAS and (b) 13C CP MAS NMR spectra of Si-Beta and Sn-containing Beta zeolites recorded after adsorption of TMPO and 2-13C-acetone, respectively. (c) 1H MAS NMR or difference spectra of various dehydrated Sn-containing Beta zeolites recorded before and after adsorption of ammonia (Reproduced from Ref. [
