一种用于光诱导反应体系的原位NMR装置的设计与应用

沈志强, 邓亚博, 杨培菊, 胡霄雪, 黄晓卷, 许传芝, 宋焕玲

Design and Application of an in situ NMR Device for Light-Induced Reaction Systems

SHEN Zhiqiang, DENG Yabo, YANG Peiju, HU Xiaoxue, HUANG Xiaojuan, XU Chuanzhi, SONG Huanling

图10 表面处理后NMR样品管对光化学诱导的动态核极化影响. (a)喷漆处理对增敏倍率的影响趋势柱状图；(b)喷漆处理NMR样品管实物图；(c)喷砂处理对增敏倍率的影响趋势柱状图；(d)喷砂处理NMR样品管实物图

Fig. 10 Effect of surface-treated NMR tubes on photochemically induced dynamic nuclear polarization. (a) histogram of the trend of the effect of paint spraying on sensitization; (b) picture of paint sprayed NMR tubes; (c) histogram of the trend of the effect of sandblasting on sensitization; (d) picture of sandblasted NMR tubes