一种用于光诱导反应体系的原位NMR装置的设计与应用
Design and Application of an in situ NMR Device for Light-Induced Reaction Systems
一种用于光诱导反应体系的原位NMR装置的设计与应用 |
| 沈志强, 邓亚博, 杨培菊, 胡霄雪, 黄晓卷, 许传芝, 宋焕玲 |
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Design and Application of an in situ NMR Device for Light-Induced Reaction Systems |
| SHEN Zhiqiang, DENG Yabo, YANG Peiju, HU Xiaoxue, HUANG Xiaojuan, XU Chuanzhi, SONG Huanling |
| 图11 原位光反应器与NMR谱仪的协同工作验证和反应前后局部信号变化谱图. (a)光促开环反应的反应历程1H NMR叠加图；(b)局部1H NMR信号变化立体化堆叠图；(c)反应前后局部1H NMR信号变化谱图 |
| Fig. 11 Validation of synergistic work of in situ photoreactor and NMR spectrometer, and spectra of local signal changes before and after the reaction. (a) Reaction course 1H NMR iterogram of the photopromoted ring-opening reaction; (b) localized 1H NMR signal change stack plot; (c) localized signal change spectrum before and after the reaction |
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