Chinese Journal of Magnetic Resonance ›› 1991, Vol. 8 ›› Issue (3): 283-290.

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NUCLEAR MAGNETIC RESONANCE STUDIES OF GINSENOSIDE Ⅰ. Structure Elucidation of an Ocotillol-Type Saponin Separated From the Leaves of Panax Quinquefolium L

Yang Yanwu1, Xu Xiaolong1, Qiu Jianqing1, Wang Dehua1, Qian Baogong1, Ma Xingyuan2, Xu Jingda2   

  1. 1. Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics, the Chinese Academy of Sciences;
    2. Department of organic chemistry, bethune University of Medical science
  • Received:1990-09-07 Revised:1990-12-04 Published:1991-09-05 Online:2018-01-20

Abstract: In this paper, 2D long-range 13C-1H heteionuctear chemical shift correlation spectroscopy, in combination with 13C-1H heteronuclear chemical shift spectroscopy and 1H-1H homonuclear chemical shift spectroscopy, have been used to elucidate the structure of an ocotillol-type saponin (OTS) which was first separated from the leaves of Panax Quinquefolium L., and the results were also confirmed by element analysis and FAB-MS techniques.

Key words: Structure elucidation, Ocotillol-type saponin (OTS), 2D-NMR, Leaves of Panax Quinquefolium L