THE 13C NMR SPECTRAL STUDIES OF SOME ATISANE TYPE DITERPENE DERIVATIVES

Chinese Journal of Magnetic Resonance ›› 1992, Vol. 9 ›› Issue (3): 277-282.

Previous Articles Next Articles

THE ¹³C NMR SPECTRAL STUDIES OF SOME ATISANE TYPE DITERPENE DERIVATIVES

Ding Yili¹, Liu Yuting²

1. Xinjiang Institute of Chemistry, The Chinese Academy of Sciences;
2. Chemistry Department, Xinjiang University, Wulumuqi 830046

Received:1991-06-22 Revised:1991-10-17 Published:1992-09-05 Online:2018-01-20

Abstract

Abstract: The chemical shifts of the ¹³C NMR and ¹H NMR spectra of eight atisane type diterpenes and one kaurane type diterpenc isolated from Euphorbia sieboldiana were assigned by their ¹³C-¹H COSY, ¹H-¹H COSY and ¹H-¹H NOESY spectral studies, and the difference of ¹³C NMR chemical shifts between atisane diterpenes and kaurane diterpenes was found, which can be used to distinguish the atisane skeleton from kaurane skeleton easily.

Key words: Atisane diterpenes, Kaurane diterpenes, 2D NMR, Euphorbia sieboldiana

Ding Yili, Liu Yuting. THE ¹³C NMR SPECTRAL STUDIES OF SOME ATISANE TYPE DITERPENE DERIVATIVES[J]. Chinese Journal of Magnetic Resonance, 1992, 9(3): 277-282.

[1]	LI Yujiang, ZHAO Wei, TAO Le, LU Bohua, ZHENG Guo, ZHANG Haiyan, GUO Xiaohe, ZHAO Tianzeng. NMR Data Analysis of Acarbose [J]. Chinese Journal of Magnetic Resonance, 2025, 42(2): 184-194.
[2]	ZHANG Rong,WANG Wei,GAO Yi,LIU Caiguang,WANG Zhenlin,QIN Yingyao,ZHANG Gong. Sensitivity Analysis of T₂-T₁ 2D NMR Measurement Parameters in Shale Oil Reservoirs [J]. Chinese Journal of Magnetic Resonance, 2023, 40(2): 122-135.
[3]	Zhen-lin WANG, Rong ZHANG, Ni ZHANG, Jing-qi LIN, Ying-yao QIN, Gang CHEN, Gong ZHANG. A High-precision Processing Method of Two-dimensional NMR Logging Data Based on Component Compensation [J]. Chinese Journal of Magnetic Resonance, 2022, 39(2): 174-183.
[4]	LI Yu-jiang, ZHAO Wei, GUO Xiao-he, TAO Le, ZHANG Xiang, ZHANG Hai-yan, ZHAO Tian-zeng. NMR Data Analysis of Manidipine Hydrochloride [J]. Chinese Journal of Magnetic Resonance, 2021, 38(1): 110-117.
[5]	LI Ying-jun, YANG Hong-jing, LIU Ji-hong, JIN Kun, LIN Le-di, LIU Xue-jie. Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative [J]. Chinese Journal of Magnetic Resonance, 2020, 37(4): 496-504.
[6]	WANG Si-hong, ZHANG Jing-dong, YIN Xiu-mei, LI Dong-hao, KAN Yu-he, HU Wei. NMR Assignments of 6-(4-chlorophenoxy)-tetrazolo[5,1-a]phthalazine [J]. Chinese Journal of Magnetic Resonance, 2020, 37(3): 390-398.
[7]	HOU Ke-jun, WU Jian-meng, GE Xiang, ZHANG Shi-mao. Calculating Porosity From Two-Dimensional NMR Relaxation Spectra of the Leikoupo Group's 4th Section [J]. Chinese Journal of Magnetic Resonance, 2020, 37(2): 162-171.
[8]	ZHANG Shi-mao, ZHANG Shao-nan, GE Xiang, WU Jian-meng. Optimal Design and Application of Two-Dimensional NMR Logging in Chuanxi Tight Gas Reservoir [J]. Chinese Journal of Magnetic Resonance, 2018, 35(2): 234-242.
[9]	ZHANG En, CUI De-yun, SUN Wei, LI Peng-yun, XU Jin-mei, LIU Hong-min. Structural Elucidation of a Hydrolysis Product from Derivatives of Allofuranose [J]. Chinese Journal of Magnetic Resonance, 2017, 34(2): 183-190.
[10]	WANG Ming，WANG Min-chang*，ZHAO Xiao-jing，SU Peng-fei，PAN Qing，CHEN Zhi-qun，LI Xiao-yu. NMR Characteristics and Crystal Structure of Cytarabine HepDirect Prodrug MB07133 [J]. Chinese Journal of Magnetic Resonance, 2015, 32(3): 518-527.
[11]	WU Xiang-yu1,2，LI Ning1,2，TANG Hui-ru1. Quantitative Analysis of Metabolites in Mungbean (Vigna Radiata*) Extracts using NMR Techniques [J]. Chinese Journal of Magnetic Resonance, 2014, 31(4): 548-563.
[12]	AN Zhi-min，MA Er-qian，YANG Qiu-qing*. Structural Changes of 2-Keto-L-Gulonic Acid Studied by NMR Spectroscopy [J]. Chinese Journal of Magnetic Resonance, 2014, 31(3): 407-414.
[13]	NIU Qiang1,2，WANG Zhi-zhan3，ZENG Jian-hui1，WANG Xin2，DU Huan-fu2，GAI Shan-shan2*. Evaluating Shale Porosity and Oil Content with 2D NMR [J]. Chinese Journal of Magnetic Resonance, 2014, 31(2): 206-213.
[14]	AN Yan-peng1,2，YANG Xiao-yan1,2，LI Hong-de1,2，LI Ning1,2，TANG Hui-ru1* . NMR Analysis of Nicotinamide N-Oxide and Pseudouridine in Rat Urine [J]. Chinese Journal of Magnetic Resonance, 2014, 31(2): 232-242.
[15]	ZHU Xin-shu1,2，CUI Jia-tao1,2，FENG Yin-gang1，ZHANG Jing-tao1，CUI Qiu1,3 . Metabolomic Analysis of Clostridium thermocellum [J]. Chinese Journal of Magnetic Resonance, 2014, 31(2): 243-252.

THE ¹³C NMR SPECTRAL STUDIES OF SOME ATISANE TYPE DITERPENE DERIVATIVES

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments