Chinese Journal of Magnetic Resonance ›› 1998, Vol. 15 ›› Issue (3): 285-289.

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THE STUDIES ON2D NMR SPECTRA OF TWO CHROMONE DERIVATIVES

Yi Yijun1, Yang Dalong1, Cao Zhengzhong1, Cao Yuan1, Wu Yongping1, Zhao Shouxun2   

  1. 1. Jiangsu Province Institute of Materia Medica, Nanjing 210009;
    2. China Pharmaceutical University, Nanjing 210009
  • Received:1997-12-01 Revised:1998-01-19 Published:1998-06-05 Online:2018-01-13

Abstract: The structures of two flavones, 5,7-dihydroxy chromone 3-0-α-L-rhamnoside(1) and 7,6'-dihydroxy 3'-methoxylisofavone (2), isolated from Smilax glabra were studied by 2D NMR spectra analyses. The attached positions of substituted groups in 1 and B ring of 2 can be determined by illustrating the COLOC and 1H-1H COSY spectra. All the proton and carbon signals of 1 were assigned in detail also.

Key words: Smilax glabra, Chromone, Isoflavone, 2D NMR, COLOC