Chinese Journal of Magnetic Resonance ›› 2006, Vol. 23 ›› Issue (2): 193-198.

• Articles • Previous Articles     Next Articles

Characterization of Phthalazinone Moiety Containing Methoxyl Side Group by NMR Spectroscopy

  

  1. State Key Laboratory of Fine Chemicals; 2.Department of Polymer Science & Materials, Dalian, 116012
  • Received:2005-09-08 Revised:2005-11-16 Published:2006-06-05 Online:2006-06-05
  • Supported by:

    国家自然科学基金资助项目(50143013).

Abstract:

The structure of 4-(3-methoxyl-4-hydroxyphenyl)-phthalazin-1-one(OO-DPHZ) was  determined by NMR spectroscopy and MS spectrometry. The 1H and 13C chemical shifts of the compound were assigned using two dimensional NMR spectroscopy, including gCOSY, gHSQC and gHMBC.

Key words: NMR spectroscopy, phthalazinone, methoxyl group, assignment, MS spectrometry

CLC Number: