Chinese Journal of Magnetic Resonance ›› 1998, Vol. 15 ›› Issue (6): 547-550.

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NMR STUDIESON 1-(2-CARBOXYBENZOYL) THIOSEMICARBAZIDE AND ITSCOPPER(I) COMPLEX

Wu Daxu, Shen Xu   

  1. State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002
  • Received:1998-04-20 Revised:1998-06-01 Published:1998-12-05 Online:2018-01-17

Abstract: In this paper 1H-1H COSY, 1H-13C HMQC and HMBC 2D NMR techniques were used to analyze and assign the 1H and 13C NMR spectra of a new ly synthesized compound 1-(2-carboxy benzoyl)-thiosemicarbazide(H3L), The 1H、13C NMR spectra of its copper (I) complex [Cu2(H3L)2Cl2](H2O)3 have also been measured.Its coordination property is briefly discussed, and the structure of the complex is suggested.

Key words: 1-(2-carboxybenzoyl)-thiosemicarbazide(H3L), Copper(I) complex, NMR