Chinese Journal of Magnetic Resonance ›› 1994, Vol. 11 ›› Issue (2): 119-126.

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NMR STUDIES OF PYRIDINE -ENSOLUBLE SOLID OF VIBRAIN AND ITS HYDROCRACKING PRODUCTS

Yang Baolian1, Li Liyun1, Ye Chaohui1, Zhang PengZhou2, Xu Xiufeng2   

  1. 1. State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wulian Institute of Physica, The Chinese Academy or Sciences, Wuhan 430071;
    2. Shanxi Institute of Coal Chemistry, The Chinese Academy of Sciences, Taiyuan 030001
  • Received:1993-05-17 Published:1994-06-05 Online:2018-01-20

Abstract: Pyridine -insoluble、THF-insoluble solids of bydrocrachng products of vitrain pyridine-insoluble solid and itself were investigated by solid state 13C CP/MAS NMR technique.From the measurements, twelve structural parameters of carbon skeleton were obtained Benzene-soluble subfraction of hydrocracking products were investigated by one and two dimensions 1H and 13C liquid NMR techniques.Their 1H and 13C spectra were assigned.The avcrage molecular structures of these fractionswere obtained.

Key words: Vitrain, Pridine-insoluble, Hydrocracking, NMR, Average molecular structure